文献类型： 外文期刊

作者： Hu, R ¹ ; Berthion, JM ¹ ; Bodereau, I ¹ ; Fournier, J ¹ ;

作者机构： 1.LAB DEPT SARTHE,F-72004 LE MANS,FRANCE; CTR REG ETUD PROD AGROPHARMACEUT,F-49070 BEAUCOUZE,FRANCE; SICHUAN ACAD AGR SCI,CENT LAB,CHENGDU,SICHUAN,PEOPLES R CHINA

关键词： Gas chromatography mass spectrometry;Triazines;Amides;Water pollution;Solid-phase extraction

期刊名称：CHROMATOGRAPHIA （ 影响因子：2.044； 五年影响因子：1.725 ）

ISSN：

年卷期：

页码：

收录情况： SCI

摘要： A simultaneous capillary Gas Chromatographic-Mass Spectrometric (GC-MS) method is described for the determination of thirteen pesticides belonging to the triazine and amide families in water. The sample is extracted in liquid-liquid mode (dichloromethane) and then the determination of the residues is carried out by capillary gas chromatography with mass spectrometric detection in the Selected-Ion Monitoring mode (SIM). The average recoveries of spiked compounds are in the 78.4-135.4 % range between the relative low level (0.100 mu g L(-1)) and the relative high level (10.0 mu g L(-1)). The limits of detection (LOD) are in the 0.009-0.128 mu g L(-1) range. [References: 14]